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Analytical Chemistry (Laboratory)
EXP 9: GRAVIMETRIC ANALYSIS OF A METAL CARBONATE
Guide Questions (9)
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What is the advantage of using calcium chloride
solution as precipitant with other solution?
Calcium chloride is effective because it reacts readily with
carbonate
ions
to form a
solid
precipitate
of calcium carbonate.
What is the advantage of using calcium chloride
solution as precipitant with other solution?
These are easy to
filter
and weigh
accurately
.
List three possible sources of error that would
cause the molar mass of the unknown to be:ately.
Too
high
Incomplete
drying of the precipitate
Contamination
with other compounds
Excess calcium chloride causing
unreacted
material in the precipitate.
List three possible sources of error that would
cause the molar mass of the unknown to be:
Too
low
Loss of
precipitate
during filtration
Insufficient
precipitation due to incorrect pH
Incomplete
reaction
How could you improve this experimental
procedure to reduce the likelihood of error?
Explain.
Ensure complete
precipitation
by controlling
pH.
How could you improve this experimental
procedure to reduce the likelihood of error?
Explain.
Thoroughly wash and dry the
precipitate
to remove
impurities
and
moisture.
How could you improve this experimental
procedure to reduce the likelihood of error?
Explain.
Handle the precipitate carefully to avoid
loss
during
filtration.