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Analytical Chemistry (Laboratory)
EXP 9: GRAVIMETRIC ANALYSIS OF A METAL CARBONATE
Procedure (9)
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Ysha Javier
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Cards (9)
Measure 2.0000 – 2.5000g of a known Group 1
metal carbonate and accurately record the mass of
the sample. What step is this?
1st
Add about 100mL of water and stir to completely
dissolve the metal carbonate. What step is this?
2nd
Allowing for the metal carbonate to be the limiting
reactant in the experiment, calculate the amount of
0.1 M CaCl₂ solution that will be added to the
reaction. What step is this?
3rd
Slowly add the calculate volume of 0.1 M CaCl₂ to
the sample solution and let the
precipitate
settle (> 5 minutes). What step is this?
4th
Filter the solution through a filter paper whose
constant weight
has been initially obtained. What step is this?
5th
Take the
filter paper
out of the funnel and place it in
the oven. What step is this?
6th
Be careful not to tear the paper or lose any part of
the solid. What step is this?
7th
Dry the filter paper at 105°C for
1 hour
. What step is this?
8th
Obtain the constant weight of the
filter paper
. What step is this?
9th