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Analytical Chemistry (Laboratory)
EXP 7: GRAVIMETRIC ANALYSIS OF A HYDRATE
7 Guide Questions
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Ysha Javier
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Cards (20)
What is water of crystallization?
Water molecules that are chemically bound within a
crystal structure
.
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Why is water of crystallization important?
It is essential for maintaining the crystal's
shape
and
stability.
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What is water of constitution?
Water
chemically
bonded within a molecule, released during a chemical reaction.
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When is water of constitution released?
When the compound undergoes a
chemical
reaction,
such as during
decomposition
.
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What is adsorbed water?
Water that is
physically bound
to the surface of materials through
weak
forces.
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How is adsorbed water held to materials?
Through weak forces, such as
van der Waals forces
, without forming a chemical bond.
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What is sorbed water?
A general term for water held on or
within
a
substance
.
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What are the two ways sorbed water can be held?
Through
adsorption
(surface-bound) or
absorption
(penetrated within the material).
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What is occluded water?
Water trapped within
pores,
cavities,
or
voids
inside a solid material.
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How is occluded water different from other types of water?
It is
physically
confined but not
chemically
bound.
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Why is it important to heat and cool the crucible and sample to room temperature before weighing?
It ensures
accurate
measurements
and prevents
distortion
of balance readings.
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What can hot objects create that affects weighing accuracy?
Air
currents
that can distort the balance readings.
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What does cooling prevent during weighing?
Thermal expansion
, which could lead to
incorrect
mass
values.
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If a hydrate is not heated sufficiently, what happens to the percent water calculated?
The percent water calculated would be
too
low.
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Why would the percent water be too low if the hydrate is not heated sufficiently?
Remaining water adds extra mass to the sample, making
mass loss
seem smaller.
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What are some systematic errors encountered in the experiment?
Incomplete
removal of water,
contamination
,
inaccurate weighing
, and
loss of sample
.
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How can contamination affect the experiment?
It can lead to
inaccurate
measurements and results.
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What can cause inaccurate weighing in the experiment?
Residue
or
moisture
on the crucible can lead to inaccurate readings.
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What is a potential issue during handling or heating of the sample?
Loss
of
sample
during
handling
or
heating
can occur.
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For accurate weighing, the crucible and sample must be at
room
temperature
for stability.